Process of extracting and preserving the original flavors and food value of fruit juices



A118 8 1950 E. G. HuzENLAuB 2,517,569

PRCESS OF EXTRACTING AND PRESERVING THE ORIGINAL FLAVORS AND FOOD VALUE 0F FRUIT JUICES Filed Nov. 23, 1945 u www, u

Patented Aug. 8, 1950 UNITED STATES PATENT CFFICE PROCESS OF EXTRACTING AND PRESERV- ING THE ORIGINAL FLAVORS AND FOOD "ALUE OF FRUIT JUICES Erich Gustav Huzenlailb, Brentford, England Application November 23, 1945, Serial No. 630,531

My invention relates to a process of extracting .nd preserving the original flavors and food value .f fruit `juices.

Fruit juices, and particularly orange juice, are in great public demand largely because of their health giving properties. Oranges are bulky, heavy, and perishable, and the orange groves are remote from most of the large centers of population. Transportation of oranges is expensive and extraction of the juice in homes and restaurants is a tedious and time-consuming chore. The juice extractable from an orange constitutes only a part of its total bulk and weight and the numerous advantages of extracting and canning the juice at or near the orange groves has long been recognized. Many attempts have been made to develop a satisfactory process for extracting and preserving orange juice, and canned orange juice is now on the market, but its taste is so. diierent from fresh orange juice that the canned juice is not acceptable to a large part of the public despite lower cost and greater convenience.

An object of my invention is to provide a new and improved process for extracting and preserving the original flavors and food value of orange juice and the juices of other fruits and vegetables.

Another object of my invention is to provide a new and improved process for extracting and preserving fruit and vegetable juices which is economical and can be carried out by persons of ordinary skill in the field of food processing.

Another object of my invention is to provide new and improved apparatus for performing the process.

Other objects and'advantages will become apparent as the description proceeds.

In the drawings, Fig. l is a diagrammatic representation of a preferred form of apparatus for carrying out my new and improved process; and

Fig. 2 is a sectional view taken on the line 2`2 of Fig. 1 and showing a detail of the screw conveyor andsealing means for disposing of the pulp or other waste product.

Fig. 3 4is -a detail view in cross section of the I upper portion of the discharge pipe from the juice-'extracting compartment shown in Fig. 1.

In Fig. 1, I have illustrated a compartment l in which the extraction of the juice is effected, this compartment having walls l2 of glass, plastic, or other suitable non-oxidizing material. The compartment I0 is connected by a pipe I4 with a source of Vacuum whereby a high vacuum such as 271/.; inches of mercury or more is main- 8 Claims. (Cl. 99-155) tained in the extracting compartment I0 during operation of the apparatus. It will be understood that the walls I2 are properly constructed and supported to withstand the differential pressure resulting from the vacuum maintained in the compartment.

The oranges are fed into the extracting compartment I0 through a pipe or duct I6 provided with one or more vacuum locks of any known or suitable construction. Such vacuum locks are shown as comprising a plurality of chambers I8 separated by doors 20. Each chamber is provided with one or more pipes 22 and valves 24 whereby air can be independently admitted or exhausted from each chamber as is well undeI-, stood in the art. Oranges discharged from the lowermost chamber I8 enter the extracting compartment I0 and fall upon the extracting rollers 26 and 28, each of which has a hollow metal core 3D surrounded by a corrugated sleeve 32 of enamel, glass, plastic, or other non-oxidizing material.

The rollers 26 and 28 are driven by shafts 3l and 36 respectively, and these shafts may have a center core of metal surrounded by non-oxidizing material and are preferably mounted so that the corrugated rollers may be moved toward and from each other to provide a ine adjustment therebetween. It is to be understood that the rollers and shafts need not have a metal core butv may be made completely of non-oxidizing material, it being essential only that no part of the rollers or shafts exposed to contact with the fruit or `juice thereof be formed of metal or other oXi-' dizing material. Suitable packing is provided at the points where the shafts project through the walls i2 of the compartment lil to prevent leakage of air into the compartment around these shafts.

The rollers 26 and 28 are preferably adjusted so that as these rollers turn in opposite directions as indicated by the arrows in Fig. 1, the ridges of the two rollers come opposite each other and cut the skin and pulp of the oranges into elongated strips as the oranges pass therethrough. The squeezing of the oranges between the rollers and the cutting action of these rollers extracts the juice from the oranges and this juice, and the skin, pulp and seeds, fall on an inclined screen 38. The recessed portions of the rollers 26 and- 3 of the recess of the opposite roller is approximately equal to the double thickness of the orange skin passing therebetween. Stationary brushes 48 are preferably provided to remove all skin and pulp from the rollers 26 and 28.

The screen 38 is provided with openings which permit only the juice to pass therethrough. The lower side of the screen 38 is subjected to a gentle bombardment by balls 42 mounted in recesses provided in a reciprocating frame 44. The frame is supported at one end by a rod 46. and the other end of this frame is supported and reciprocated by a crank 48. The bombardment of the screen 38 prevents clogging of the screen so that the orange juice can pass therethrough, and causes the skin, pulp, seeds and other waste matter to slide down the screen into the housing I of a screw conveyor 52. The juice passing through the screen 38 flows into an inclined trough 54 leading to discharge pipe 56 communicating with the compartment I8 at a lower portion thereof.

The screw conveyor 52 is of the pressureand seal-forming type and includes a rotating screw I8 which forces the skin, pulp, seeds, and any other refuse material into a contracting tube 68 which extends through a wall of the extracting compartment and has its discharge end located above a receptacle 62 or other means into which the waste material is discharged. It will be understood by those skilled in the art that the screw conveyor packs the Waste material into the tapered tube with suflicient firmness to form a vacuum seal so that air cannot enter the extracting compartment through this tube. While I have referred to the orange skins, pulp, and seeds as waste material, this material has value as an ingredient of animal feed and constitutes a byproduct of my process.

The screen 38, balls 42, frame 44, rod 46, crank 48, housing 58, trough 54, and screw 58, as well as all other parts of the apparatus with which the orange juice comes in contact or can come in contact, are partly or wholly formed of non-oxidizing material and present only a non-oxidizing surface so that at no time in the operation of my process does the orange juice come in contact with any metal or other oxidizing material. The pipe 56 and tank 64 into which it discharges are likewise formed wholly of or are lined with nonoxidizing material. For convenience this pipe 56 will be considered as consisting of an upper and enlarged portion 66, an intermediate portion 68, and a. lower portion 10, al1 of which are normally lled with orange juice during the operation of the apparatus.

The oranges shouldbe washed before depositing them in the duct I8 leading to the extraction compartment I8, and the oranges should be inspected also, and all spoiled or rotten oranges removed. However, some dirt and spoiled oranges will find their way into the extracting compartment I8, and it is usually necessary and desirable therefore to sterilize the orange juice before bottling it. This sterilization could be accomplished in various ways, but is most effectively done by means of frequencies within the infrared range. A preferred method of application is .by means of the magnatype lamps 12 arranged one above the other and surrounding the intermediate portion 68 of the pipe 56. The orange juice in this intermediate portion of the pipe is preferably heated to between 225 to 230 F. for a period of ten minutes or more.

Any vapor resulting from such heating tends to be absorbed by the orange juice in the upper portion of the pipe 56 and in the compartment I8, and it is desirable to prevent the temperature of the juice in the upper portion to rise above the corresponding boiling point of the vacuum employed. Upper portion 66 of the pipe' is therefore made of sufficient volume so that any vapor produced in the central portion 68 will be cooled and converted to liquid before reaching the upper end of the pipe 56. The lower portion 18 is pro vided with a cooling jacket I4 of any suitable type but illustrated as having a water inlet 16 and a water outlet 'I8 and effective to cool the orange juice before it enters the tank 64. As an example of the proper length and size of the several portions of the pipe 56, upper portion 66 could be sixteen feet, the intermediate or heating portion 68 ten feet, and the cooling portion 18 ten feet, but it is to be understood that these figures are illustrative only and that other lengths could be utilized. It is important, however, that the upper portion 66 have a capacity of six to eight or more times that of heating portion 68 and be of sumcient length so that no vapor reaches the compartment I8.

The tank 64 has an outlet 88 located in a filling and capping compartment 82 which is connected with a Source of vacuum by way of pipe 64 and valve 86. Suitable valve mechanism 88 controls the discharge of the orange juice into glass bottles 98 or other suitable containers which are moved to a position beneath the outlet 88 by a conveyor 92 having upwardly extending ribs 94 against which the bottles rest. These ribs serve properly to space the bottles lengthwise of the conveyor for movement through the compartment 82 and vacuum locks on each side thereof.

Before entering the filling compartment 82 each bottle must pass through a plurality of vacuum locks 96 illustrated as consisting of two cham-- bers, each provided with a pipe 98 and valve 188 whereby the pressure in a chamber can be individually controlled. Doors l82 separate the vacuum chambers from each other and also from filling compartment 82 and from atmosphere. After a bottle has been filled, a capping mechanism |84 of any usual construction applies a crown seal or other closure thereto. The capping mechanism is located in the evacuated filling compartment 82 and it will 'be understood that all of the walls of this compartment as well as all exposed parts of the valve mechanism 88 and capping mechanism |84 are of non-oxidizing inaterial. The filled and capped bottles leave the filling compartment by way of a second set of vacuum locks |86. The number of vacuum locks may be varied as desired and instead of sealing the orange juice in bottles, the orange juice may lbe put up in metal cans or any other suitable containers provided that the metal inner surface of the cans or other containers are coated with material which is non-oxidizing and which does not react with any ingredient of the orange juice.

In carrying out my novel process, the oranges are preferably first Washed and inspected, and all rotten oranges removed before the remaining oranges are put into the upper end of the duct 'i8 or any suitable hopper which may be connected therewith. The uppermost chamber i8 of the vacuum locks is then exposed to atmosphere and thereafter the door which separates this chamber.- from the hopper is opened to permit the oranges to fall into the chamber. This chamber is then evacuated and the door 28 which separates this chamber from the next chamber therebelow is opened to permit the oranges to fall into the lower -the juice.

V short interval, for further evacuation ci' air the door which separates this chamber from the chamber therebelow is opened and the oranges dropped into the latter chamber. This step by step movement of the oranges through the vacuum chambers is continued until the oranges are discharged onto the rollers 26 and 28 in the extracting compartment I0.

Rotation of these rollers squeezes the oranges therebetween and cuts the skin and pulp into strips.

During this operation the juice is extracted from the oranges and a certain amount of oil is extracted from the `orange skins. The oill extracted from the orange skins mixes with the juice but is insulcient in amount to alter the flavor of In fact, the presence of a small amount of 'this oil in the juice appears to be beneficial in preserving the original iiavor and food value of the juice. The mixture of oil and orange juice is hereinafter referred to merely as orange juice.

The juice, pulp, skin and seeds fall on inclined screen 38, and the brushes 4U prevent any of this material from adhering to the extracting rollers. Bombardment of the screen 38 by the rubber balls 42 prevents clogging of the screen and facilitates the passage therethrough of the orange juice. The waste material, that is, the skin, pulp, and seeds, travels down the screen into the conveyor 52. The conveyor screw forces the waste material into the tapered tube E and because the skin and t pulp have been cut into strips, the conveyor screw can and does pack the waste material into the tapered tube 60 tightly enough to provide an ef- Iective air seal which prevents the entry of air into the extracting compartment i0. The waste material is discharged into the container 62 or onto a travelling conveyor as may be desired.

While the vacuum locks through which the oranges'enter the extracting compartment l0 prevent any appreciable amount of air from entering this compartment with the oranges, the oranges themselves contain air and I have provided means for removing all of this air from the orange juice. As the orange juice is extracted by the rollers 2B and 28 and passes through the screen 38, it is exposed to the vacuum in the compartment l0 and during this time air entrained in the juice has an opportunity to escape therefrom. To insure complete elimination of ain' however, the juice is also exposed to the high vacuum while it remains in the compartment ld and under conditions favorable to the removal oi air from the juice, i. e. with a large exposed surface. The rate of operation of the apparatus is such that a period of at least one minute ensues between the time the orange juice is extracted by the extracting rollers and the time that this juice enters the upper end oi the pipe 56, and during this entire time the conditions are such that any air entrained in the juice can escape therefrom and be drawn oif by the vacuum .producing means. While the shape and arrangement of the extracting compartment and the mechanism therein can be varied within wide limits, and other separating means such as a centrifuge can be used in lieu of the screen 38, I have found it desirable to expose the orange juice to a high vacuum for at least one minute under conditions which will facilitate the removal of air from the juice before the juice is bottled or sealed in other types of containers.

As the juice slowly feeds downwardly in this pipe 56, it is first exposed to vapors driven of! from juice therebelow by the heating means 12.

none o! these vapors reach theextracting com-` partment l0. When the orange juice reaches the pipe section 68, it is exposed to the action of the heating means 12. These means heat and sterilize the juice and possibly have other advantageous actions thereon. The juice is then cooled in the lower section of the pipe 1l! surrounded by the water jacket 14 and thereafter passes into the tank 8l. From the tank 84 the juice is discharged into glass bottles or other containers having nonoxidizing inner surfaces and sealed therein under high vacuum.

The bottles are evacuated before entering the filling compartment and are sealed before leaving this compartment. Throughout the entire process the juice is protected against contact with air, metal. and other oxidizing material, so that not even as much as a screw head of oxidizing material is ex-posed to the orange juice. This protection of the orange juice against air and oxidizing material and the blending of juice with the proper amount of oil from the skin produces a juice which retains all its natural flavors vand nutritional characteristics.

While I have described my invention as being used to extract and preserve orange juice, my invention is not limited to such use but is capable of general application to the extraction and preservation of fruit and vegetable juices. Likewise .I have illustrated only a single embodiment of my novel apparatus and it is to be understood that this apparatus may be widely varied to satisfy different conditions of operation both in the ex traction and preservation oforange juice and in the extraction and preservation of the juices ot other fruits and vegetables. My invention includes al1 variations, modifications, and alterna tives coming within the scope of the appended claims.

I claim:

l. The method of extracting fruit and vegetable juices and preserving the original flavors and food values thereof which comprises, cutting the foodstuff into strips under a high vacuum, squeez ing the juice from the pulp Without substantially disintegrating the pulp and skins, separating the juice from the waste skin strips, pulp and any seeds, discharging said waste, the skin strips serving as packing means during the discharging step to prevent lessening of the vacuum, and the vacuum serving to extract air dispersed in the juice and to prevent air from later coming in contact therewith, forming, under the same high vacuum, a moving column of said juice, said column comprising at a given moment an upper portion, an intermediate portion and a lower portion, the upper portion comprising a volume at least about six times the volume of the intermediate portion, heating said intermediate portion of juice to sterilize the same, permitting any vapor formed during the heating step to condense in the juice comprising said upper portion, introducing sterilized and cooled juice from the lower portion of the column into a container and sealing the juice therein, permitting heated juice in the intermediate portion to form a succeeding lower portion and cooling the same, replacing the theretofore intermediate portion of juice by `juice from the upper portion, replenishing the upper portion with new juice, and repeating the foregoing steps-protecting the .juice against contact with air and oxidizing material atY all times from the beginning of the extracting operation until the sealed containers are opened.

2. 'Ihe method as defined in claim 1, wherein the respective lengths of the several portions of the column of juice are: Upper portion, about sixteen feet; intermediate portion, about ten feet; and lower portion, about ten feet.

3. The method as deiined in claim 1, wherein the intermediate portion of the column `of juice is heated to a temperature between about 225 and about 230 F. for at least ten minutes by radiant energy within the infrared range.

4. The method as defined in claim 1, wherein the volume of the upper portion of the column of juice is from about six times to about eight times the volume of the intermediate portion thereof.

5. The method of extracting orange juice and preserving the original avor and food value thereof which comprises cutting oranges into strips under a high vacuum, squeezing the juice from the pulp and some oil from the skins without substantially disintegrating the pulp and skins, mixing the oil and juice, separating the mixed orange juice from the waste skin strips` pulp and any seeds, discharging said waste, the skin strips serving as packing means during the discharging step to prevent lessening of the vacuum, and the vacuum serving to extract air dispersed in the orange juice and to prevent air from later coming in contact therewith, forming, under the same high vacuum, a moving column of the orange juice, said column comprising at a given moment an upper portion, an intermediate portion and a lower portion, the upper portion comprising a volume at least about six times the volume of the intermediate portion, heating said intermediate portion o1 orange juice to sterilize the same, permitting any vapor formed during the heating step to condense in the juice comprising said upper portion, introducing sterilized f Number and cooled orange juice from the lower portion of the column into a container and sealing the juice therein, permitting heated juice in the intermediate portion to forma succeeding lower portion and cooling the same. replacing the theretofore intermediate DOrtion of juice by juice from the upper portion, replenishing the upper portion with new juice, and repeating the foregoing steps,protecting the orange juice against contact with air and oxidizing material at all times from the beginning of the extracting operation until the sealed containers are opened.

6. The method as dened in claim 5, wherein the respective lengths of the several portions of the column of orange juice are: Upper portion, about sixteen feet; intermediate portion, about ten feet; and lower portion, about ten feet.

7. The method as defined in claim 5, wherein the volume of the upper portion of the column of orange juice is from about six times to about eight times the volume of the intermediate portion thereof.

8. The method as dened in claim 5, wherein the intermediate portion of the column of orange juice is heated to a temperature between about 225 and about 230 F. for at least ten minutes by radiant energy within the infrared range.

ERICH GUSTAV HUZENLAUB.

REFERENCES CITED UNITED STATES PATENTS Name Date Ryan May 9. 1918 Kellogg June 27, 1916 Manning Oct. 2, 1928 Kokatnur June 4, 1929 Maull Sept. 5, 1933 Grindrod Nov. 3, 1936 

1. THE METHOD OF EXTRACTING FRUIT AND VEGETABLE JUICES AND PRESERVING THE ORIGINAL FLAVORS AND FOOD VALUES THEREOF WHICH COMPRISES, CUTTING THE FOODSTUFF INTO STRIPS UNDER A HIGH VACUM, SQUEEZING THE JUICE FROM THE PULP WITHOUT SUBSTANTIALLY DISINTEGRATING THE PULP AND SKINS, SEPARATING THE JUICE FROM THE WASTE SKIN STRIPS, PULP AND ANY SEEDS, DISCHARGING SAID WASTE, THE SKIN STRIPS SERVING AS PACKING MEANS DURING THE DISCHARGING STEP TO PREVENT LESSENING OF THE VACUM, AND THE VACUUM SERVING THE EXTRACT AIR DISPERSED IN THE JUICE AND TO PREVENT AIR FROM LATER COMING IN CONTACT THEREWITH, FORMING, UNDER THE SAME HIGH VACUUM, A MOVING COLUMN OF SAID JUICE, SAID COLUMN COMPRISING AT A GIVEN MOMENT AN UPPER PORTION, AN INTERMEDIATE PORTION AND A LOWER PORTION, THE UPPER PORTION COMPRISING A VOLUME AT LEAST ABOUT SIX TIMES THE VOLUME OF THE INTERMEDIATE PORTION, HEATING SAID INTERMEDIATE PORTION OF JUICE TO STERILIZE THE SAME, PERMITTING ANY VAPOR FORMED DURING THE HEATING STEP TO CONDENSE IN THE JUICE COMPRISING SAID UPPER PORTION, INTRODUCING STERILIZED AND COOLED JUICE FROM THE LOWER PORTION OF THE COLUMN INTO A CONTAINER AND SEALING THE JUICE THEREIN, PERMITTING HEATED JUICE IN THE INTERMEDIATE PORTION TO FORM A SUCCEEDING LOWER PORTION AND COOLING THE SAME, REPLACING THE THERETOFORE INTERMEDIATE PORTION OF JUICE BY JUICE FROM THE 